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It was found that the use of thionyl chloride and sulfuryl chloride leads to contamination of DND-Cl samples of sulfur. it was shown that the method of gas-phase chlorination of DND with molecular chlorine at elevated temperatures is preferable when using DND in biomedical applications; this method also helps to reduce the concentration of metal impurities. It is shown that the samples of the DND-Clhave satisfactory hydrolytic stability DND.