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The manufacture of biomaterials based on calcium phosphates for bone tissue replacement is a topical issue of modern material science. The latest developments are related to the regenerative approach, which requires the investigation of highly resorbable materials based on calcium phosphates with Ca/P ratio < 1.5. The usage of non-aqueous medium for the calcium phosphate synthesis is a promising tool to avoid the impurities, eliminate water influence and gain more control of the material.