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In the course of our ongoing studies on the development of new methods for the selective introduction of CF3 groups into bioactive compounds by means of appropriate building blocks, including α-CF3-diazo compounds, herein we disclose our findings on the direct RhIII-catalyzed C-7functionalization of indolines by using methyl 3,3,3-trifluoro-2-diazopropionate as a cross-coupling partner.