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The current literature provides abundant results on the electrical double layer structure on electrodes of liquid alloys (first of all, alloys of Ga with Tl, In, Pb, Cd and certain other metals). At the same time, until very recently, the respective results on the double layer structure of solid alloys were either absent or highly contradictory. As was shown in our studies, this gap can be compensated by using the method of electrochemical measurements on electrodes of solid alloys the surface of which is periodically renewed by mechanically cutting off thin metal layers.