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Recent advances in the preparation of adsorbent layers for thin-layer chromatography combined with matrix-assisted laser desorption/ionization mass-spectrometric detectionстатья Исследовательская статья
Информация о цитировании статьи получена из
Web of Science,
Scopus
Статья опубликована в журнале из списка Web of Science и/или Scopus
Дата последнего поиска статьи во внешних источниках: 14 февраля 2019 г.
- Авторы: Kucherenko E., Kanateva A., Pirogov A., Kurganov A.
- Журнал: Journal of Separation Science
- Том: 42
- Номер: 1
- Год издания: 2019
- Издательство: John Wiley & Sons Ltd.
- Местоположение издательства: United Kingdom
- Первая страница: 415
- Последняя страница: 430
- DOI: 10.1002/jssc.201800625
- Аннотация: This review is focused on planar chromatography hyphenated with mass- spectrometric detection for analysis of low-molecular-mass solutes. Various kinds of hyphenations are discussed with attention paid to the preparation of thin layer plates suited both for the mass-spectrometric detection of the resolved solutes direct from thin-layer plates and for indirect mass-spectrometric detection of the resolved solutes, performed by scraping, extracting, purifying, and concentrating the analyte from the thin-layer chromatography plate. Plates with monolithic layers are relatively new for thin-layer chromatography but they can successfully be combined with mass- spectrometric technique in a pursuit of comprehensive local sample composition infor- mation. Preparation of monolithic layers of different porosity and structure based on organic, inorganic, and composite materials is illustrated together with examples of successful separation and detection of low-molecular-mass solutes by means of matrix-assisted and surface-assisted laser desorption mass spectrometry.
- Добавил в систему: Пирогов Андрей Владимирович
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