|
ИСТИНА |
Войти в систему Регистрация |
ИСТИНА ИНХС РАН |
||
The effects of subsonic and supersonic dissociated air flow on the surface of ultra-high-temperature HfB2-30 vol% SiC ceramics obtained using the sol-gel methodстатья
Статья опубликована в высокорейтинговом журнале
Информация о цитировании статьи получена из
Web of Science,
Scopus
Статья опубликована в журнале из списка Web of Science и/или Scopus
Дата последнего поиска статьи во внешних источниках: 14 октября 2020 г.
- Авторы: Simonenko E.P., Simonenko N.P., Gordeev A.N., Kolesnikov A.F., Lysenkov A.S., Nagornov I.A., Sevastyanov V.G., Kuznetsov N.T.
- Журнал: Journal of the European Ceramic Society
- Том: 40
- Номер: 4
- Год издания: 2020
- Издательство: Elsevier BV
- Местоположение издательства: Netherlands
- Первая страница: 1093
- Последняя страница: 1102
- DOI: 10.1016/j.jeurceramsoc.2019.11.023
- Аннотация: By hot pressing (1900 °C, 30 MPa, holding time 15 min) of HfB2-(SiO2-C) composite powder, an ultra-hightemperature ceramic material of HfB2-30 vol% SiC composition with nanocrystalline silicon carbide has been obtained. The effects of subsonic and supersonic dissociated air flow on the surface of produced materials have been studied on a high-frequency induction plasmatron in the geometry of a cylindrical sample with a flat face, fixed in a copper water-cooled holder with a 1mm protrusion. It has been shown that a sudden rise in the average surface temperature of the samples to ∼2600 °C is characteristic for both modes, which is associated with the occurrence of local sites with a temperature>2000 °C and a subsequent increase in their area. It is a matter of evaporation of the borosilicate glass layer from the surface of the oxidized sample and formation of the ceramic layer of a highly catalytic and low thermal conductive porous HfO2 layer, which is confirmed by the emission spectroscopy data, XRD and elemental analysis of the material surface after the experiments. The features of heating the oxidized surface of the samples under the impact of subsonic and supersonic dissociated air flow have been noted: there are differences in the location of overheated sites, initiating a sharp temperature rise and the rate of growth of their area
- Добавил в систему: Нагорнов Илья Алексеевич