Аннотация:A 3Ti–Si–2C composite material is obtained by self-propagating high-temperature synthesis, inwhich C60/70 fullerite is used as carbon. Its phase composition and structure are investigated by X-ray diffraction and scanning electron microscopy. It is shown that a composite containing TiC carbide, Ti5Si3Cx carbosilicide, and Ti3SiC2 MAX phase as well as traces of titanium silicide TiSi2 is formed as a result of synthesis. The structure of the samples is inhomogeneous and contains regions that simultaneously consist of several phases.