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Development of Methods of the Gas Chromatographic Determination of Phenylcarboxylic Acids in Blood Serum and their Adaptation to Clinical Laboratory Conditionsстатья
Информация о цитировании статьи получена из
Web of Science,
Scopus
Статья опубликована в журнале из списка Web of Science и/или Scopus
Дата последнего поиска статьи во внешних источниках: 5 мая 2015 г.
- Авторы: Moroz V.V., Beloborodova N.V., Bedova A.Yu, Revel’skii A.I., Getsina M.L., Osipov A.A., Sarshor Yu N., Buchinskaya A.A., Olenin A.Yu
- Журнал: Journal of Analytical Chemistry
- Том: 70
- Номер: 4
- Год издания: 2015
- Издательство: Maik Nauka/Interperiodica Publishing
- Местоположение издательства: Russian Federation
- Первая страница: 495
- Последняя страница: 501
- DOI: 10.1134/S1061934815040103
- Аннотация: A method has been developed for the determination of phenylcarboxylic acids (benzoic, p-hydroxyphenyllactic, p-hydroxyphenylacetic, phenyllactic, 3-phenylpropanoic, and phenylacetic) in blood serum by gas chromatography with a flame ionization detector (FID). The quantitative characteristics of analysis obtained with the FID and mass spectrometric detectors are in the same range and exhibit common trends for different groups of samples. It has been shown that the reproducibility of the results increases with the addition of a stage of salting out to the sample preparation procedure. The accuracy of the results is estimated using the added–found method. A possibility of the application of widely used FID to the quantitative determination of phenylcarboxylic acids in blood serum has been demonstrated for routine clinical practice.
- Добавил в систему: Оленин Андрей Юрьевич
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